Homonuclear dipolar decoupling in solid-state nuclear magnetic resonance under the regime of moderate to high magic-angle spinning frequencies:Astatus report

Subhradip Paul, P K Madhua


We review here the status of homonuclear dipolar decoupling in solid-state nuclear magnetic resonance. With the advent of probes capable of high spinning frequencies, the focus of methodology development emphasises on the applicability of the pulse sequences in the moderate to ultra-fast spinning regime. This review outlines the homonuclear dipolar decoupling sequences that have shown the potential to yield high-resolution 1H spectra at high spinning frequencies.


Solid-State NMR; Homonuclear dipolar decoupling; Lee-Goldburg; PMLG; Symmetry sequences; DUMBO; High MAS frequencies.

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